{"id":32282,"date":"2022-09-21T10:28:58","date_gmt":"2022-09-21T08:28:58","guid":{"rendered":"https:\/\/stage.muegge.de\/decontamination-of-process-water-containing-organic-residues-using-an-atmospheric-pressure-microwave-plasma-process\/"},"modified":"2022-11-28T17:24:35","modified_gmt":"2022-11-28T16:24:35","slug":"decontamination-of-process-water-containing-organic-residues-using-an-atmospheric-pressure-microwave-plasma-process","status":"publish","type":"post","link":"https:\/\/muegge-group.com\/en\/decontamination-of-process-water-containing-organic-residues-using-an-atmospheric-pressure-microwave-plasma-process\/","title":{"rendered":"Decontamination of Process Water containing Organic Residues using an Atmospheric Pressure Microwave Plasma Process"},"content":{"rendered":"\t\t
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The thermo-catalytic reforming process (TCR\u00ae process) developed through a collaboration between MUEGGE and the Fraunhofer Institute for Environmental, Safety and Energy Technology (Fraunhofer UMSICHT) produces synthetic natural gas, pyrolytic carbon, and synthetic crude oil. Process water is used in the TCR\u00ae process; after the process, the water is contaminated with organic compounds like acetonitrile, acetic acid, phenol, pyridine, and pyrroles. For the process water to be recycled, these organic compounds must be removed. MUEGGE\u2019s atmospheric pressure microwave plasma torch [1] was applied for the decontamination of process water.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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1.\tAtmospheric pressure microwave plasma setup for the decontamination of process water<\/h4>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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The decontamination of the process water was performed by Fraunhofer UMSICHT using MUEGGE\u2019s atmospheric pressure microwave plasma torch operated with air at 2.45\u00a0GHz, see Figure 1. The treatment process consists of swirling compressed air into the contaminated process water and to inject the resulted air-water flow via<\/em> a venturi nozzle into the MUEGGE 2.45\u00a0GHz plasma torch as to form tiny droplets of water [2]. The smaller the droplets of process water in the pressurized airstream, the higher the probability for complete dissociation of the organic compounds in the high-energy microwave plasma. The desirable result of this atmospheric pressure plasma cleaning process would be the complete conversion of the organic compounds into water vapor and carbon dioxide after dissociation and reaction with hydroxide- and oxygen-radicals formed within the microwave plasma.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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Figure 1: Atmospheric pressure microwave plasma setup for decontamination of process water.<\/figcaption>\n\t\t\t\t\t\t\t\t\t\t<\/figure>\n\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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At the exit of the 2.45\u00a0GHz air plasma, the decontaminated process water can be easily recaptured by rapid cooling, as shown in Figure 2.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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Figure 2: Recapturing the decontaminated process water by quenching.<\/figcaption>\n\t\t\t\t\t\t\t\t\t\t<\/figure>\n\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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To demonstrate the efficiency of the atmospheric pressure microwave plasma decontamination of process water, solutions of 8.74\u00a0g ethanol and 16.81\u00a0g acetic acid dissolved in 1\u00a0l of distilled water were used as substitutes of the organic compounds in the laboratory scale experiments performed by Fraunhofer UMSICHT.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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2.\tResults of the plasma decontamination tests using a solution of ethanol<\/h4>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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A solution of 8.74\u00a0g of ethanol in 1\u00a0l of distilled water was injected in compressed air and fed into the atmospheric pressure microwave plasma with a flowrate of 130\u00a0l\/min, which corresponds to a flowrate of approximately 65\u00a0ml\/min of the test solution. According to the results obtained by Fraunhofer UMSICHT, the proportion of ethanol dissolved in distilled water was reduced by 92% after its treatment in the air microwave plasma using 2\u00a0kW of microwave power.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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3.\tResults of the plasma decontamination tests using a solution of acetic acid<\/h4>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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A test solution of 16.81\u00a0g of acetic acid in 1\u00a0l of distilled water was added into compressed air and fed into the atmospheric pressure microwave plasma with a flowrate of 130\u00a0l\/min, which corresponds to a flowrate of approximately 65\u00a0ml\/min of the test solution. Measurements of the content of acetic acid dissolved in distilled water showed a reduction by 88% after its treatment in the air microwave plasma operated at 2\u00a0kW of microwave power.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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4.\tConclusion: Successful and efficient decontamination of the process water by atmospheric pressure microwave plasma<\/h4>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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The laboratory experimental results have shown 92% reduction of ethanol and 88% reduction of acetic acid using the atmospheric pressure air plasma at 2 kW microwave power.<\/p>\n

These preliminary results are very promising for high efficiency cleaning of process water from TCR\u00ae applications. Working at elevated microwave power levels (e.g.,<\/em> MUEGGE\u2019s 75 kW APS @ 915 MHz) will allow the removal of significantly higher quantities of organic contaminants and the process of considerably higher flows of contaminated process water.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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\u00a0<\/strong><\/p>\n

\u00a0<\/strong><\/p>\n

References<\/strong><\/p>\n

[1]\u00a0 \u00a0 \u00a0 \u00a0 M\u00fcller, Robert and Gorath, Moritz, et al.: Atmospheric Pressure Plasma Source and Downstream Source: Characteristics and Industrial Applications, Invited Talk, Contributions to 56th<\/sup> Annual Microwave Power Symposium (IMPI 56), Savannah, Georgia (USA), June 14-16, 2022.<\/p>\n

[2]\u00a0 \u00a0 \u00a0 \u00a0 Kaiser, Nadine: Behandlung von schwach kontaminierten Abw\u00e4ssern mittels Plasma-Technologie (Treatment of low-contaminated residual water using plasma technology), Bachelor\u2019s Thesis, Technische Hochschule Nuremberg \u201eGeorg Simon Ohm\u201c, August 4, 2021.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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The thermo-catalytic reforming process (TCR\u00ae process) developed through a collaboration between MUEGGE and the Fraunhofer Institute for Environmental, Safety and Energy Technology (Fraunhofer UMSICHT) produces synthetic natural gas, pyrolytic carbon, and synthetic crude oil. Process water is used in the TCR\u00ae process; after the process, the water is contaminated with organic compounds like acetonitrile, acetic […]<\/p>\n","protected":false},"author":4,"featured_media":0,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[5345],"tags":[6096,6095,768,6539],"class_list":["post-32282","post","type-post","status-publish","format-standard","hentry","category-power-to-x-applications-en","tag-microwaves","tag-mikrowelle-en","tag-muegge-blog-en","tag-plasma"],"acf":[],"yoast_head":"\nDecontamination of Process Water containing Organic Residues using an Atmospheric Pressure Microwave Plasma Process - Muegge<\/title>\n<meta name=\"description\" content=\"How Duo-Plasmaline systems open new horizons for growing marketsHow plasma technology solves the challenge of performance degradation in fuel cells\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/muegge-group.com\/en\/decontamination-of-process-water-containing-organic-residues-using-an-atmospheric-pressure-microwave-plasma-process\/\" \/>\n<meta property=\"og:locale\" content=\"en_GB\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Decontamination of Process Water containing Organic Residues using an Atmospheric Pressure Microwave Plasma Process - 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